KitAlysis™ High-Throughput Suzuki-Miyaura Cross-Coupling Reaction Screening Kit - Pack of 4
ALDRICH/KITALYSIS-SM
Synonym: Suzuki-Miyaura Cross-Coupling
Product Type: Equipment/Book
functional group | phosphine |
reaction suitability | reaction type: Cross Couplings |
reaction type: Suzuki-Miyaura Coupling | |
reagent type: catalyst core: palladium |
Application: | Screening kit for Suzuki-Miyaura cross-coupling reaction. Step-by-step user guide and a downloadable experimental excel sheets are provided in the below hyperlink. Step-by-Step Guide for Suzuki-Miyaura Cross-Coupling Reaction Screening Kit Downloadable experimental excel sheet Each kit contains 4 customizable screening sets that include the following components: • 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat. • 1 (2 mL) ampule each of Toluene, THF, n-Butanol, DMAc, and aq. 1.5 M K3PO4. • 4 NEW KitAlysis 24-Well Reaction Block Replacement Films. • 4 substrate reaction vials with stir bars. • 1 internal standard. Monitor reaction progress via TLC-MS by following this protocol Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately). |
Features and Benefits: | • Designed and tested by synthetic chemists. • Easily run 24-microscale reactions in parallel. • 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration. • Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks. |
Legal Information: | KitAlysis is a trademark of Sigma-Aldrich Co. LLC |
Symbol | GHS02,GHS05,GHS07,GHS08,GHS09 |
Signal word | Danger |
Hazard statements | H225 - H302 + H312 + H332 - H304 - H315 - H318 - H335 - H336 - H351 - H360D - H373 - H410 |
Precautionary statements | P210 - P273 - P280 - P301 + P310 - P305 + P351 + P338 - P331 |
RIDADR | UN 3316 9 |
Flash Point(F) | 1.4 °F |
Flash Point(C) | -17 °C |
Supplemental Hazard Statements | EUH019 |
UNSPSC | 12352200 |
Components | Pd-PEPPSI™-IPent catalyst, ≥95% 5 µmol; SPhos Pd G2 5 µmol; cataCXium® A Pd G2 5 µmol; XPhos Pd G3, 98%, 1:1 MTBE adduct 5 µmol; P(Cy3) Pd G3, 97% 5 µmol; APhos Pd G3, 97% 5 µmol; Toluene, anhydrous, ZerO2®, 99.8% 8 mL; Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9% 8 mL; 1-Butanol, anhydrous, ZerO2®, 99.8% 8 mL; N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8% 8 mL; Degassed Potassium phosphate tribasic solution 8 mL; Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm 1 EA; SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA |